Sodium Sulfide Nonahydrate Analytical reagent USP Grade Suppliers & Manufacturers
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Sodium Sulfide Nonahydrate
CAS Number 1313-84-4, Analytical reagent USP Grade & Pure
Sodium sulfide is the chemical compound with the formula Na2S, or more commonly its hydrate Na2S-9H2O. Both the anhydrous and the hydrated salts are colorless solids. They are water-soluble emit hydrogen sulfide, which smells like rotten eggs. Commonly available grades have around 60% Na2S by weight, which means molecular formula of Na2S-3H2O. It is used in water treatment as an oxygen scavenger agent and also as a metals precipitant; in chemical photography for toning black and white photographs; in the textile industry as a bleaching agent, for desulfurising and as a dechlorinating agent; and in the leather trade for the sulfitisation of tanning extracts. It is used in chemical manufacturing as a sulfonation and sulfomethylation agent. It is used in the production of rubber chemicals, sulfur dyes, pharmaceuticals, and other chemical compounds.
Sodium Sulfide Nonahydrate Analytical Reagent Grade Specifications
REQUIREMENTS
Na2S-9H2O --- Formula Weight 240.18
CAS Number 1313-84-4
NOTE: To enhance stability, storage below 10C is recommended.
Appearance: Crystals, colorless or with only a slight yellow color
Assay: 98.0% Na2S . 9H2O
MAXIMUM ALLOWABLE
Ammonium (NH4): 0.005%
Sulfite and thiosulfate (as SO4): 0.1%
Iron: Passes test.
Sodium Sulfide USP Grade Specifications:
Na2S-9H2O --- 240.18
Sodium sulfide nonahydrate
Disodium sulfide nonahydrate CAS 1313-84-4DEFINITION
Sodium Sulfide contains NLT 98.0% and NMT 103.0% of sodium sulfide (Na2S-9H2O).IDENTIFICATION
A.
Conduct this test in a fume hood.
Sample: 100 mg.
Analysis: To the Sample add 10 mL of 3 N hydrochloric acid and cover the top of the container with filter paper saturated with a 0.2 M lead acetate solution.
Acceptance criteria: A brownish or silvery-black color forms on the paper.ASSAY
Limit of Iron:
Acceptance criteria: 98.0% to 103.0%
Sample solution: 50 mg/mL in water.
Acceptance criteria: The solution is clear and colorless.
Limit of Sulfite and Thiosulfate:
Sample solution: Dissolve 3.0 g of Sodium Sulfide in 200.0 mL of filtered and degassed water. Add 100.0 mL of 0.2 N zinc sulfate, and allow to stand for 30 min. Filter, and add 1 mL of starch.
Titrimetric system
Mode: Direct titration
Titrant: 0.01 N iodine
Endpoint detection: Visual
Analysis: Titrate 100.0 mL of the filtrate from the Sample solution with Titrant.
Acceptance criteria: NMT 3.0 mL of Titrant is required.Sodium Sulfide Nonahydrate Analytical reagent USP Grade Manufacturers:
Muby Chem Ltd.
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